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When you pour off the solvent a little bit is remaining to the crystals but which will evaporate when it warms.. it wont be sufficient to dissolve you xtals.EDIT: I did the titration. I made use of 500ml of my inventory solution HCl, and titrated versus my inventory solution of NaOH. HCl is 0.001M and NaOH is 5M.I will do A further extraction using